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Magnetostrictive transducers are commonly used as actuators and sonar transducers, and in remote non-destructive evaluation. Their use in wireless thermometry is relatively unexplored. Since magnetostriction-based sensors are passive, they could potentially enable long-term near-field thermometry. While the temperature sensitivity of resonance frequency in magnetostrictive transducers has been reported in previous studies, the origin of the temperature sensitivity has, however, not been elucidated. this website Here, we identify material properties that determine temperature sensitivity and identify ways to improve sensitivity as well as the detection technique. Using a combination of analytical and computational methods, we systematically identify the material properties that directly influence the temperature coefficient of resonance frequency (TCF). We first experimentally measure the shift in resonance frequency due to temperature changes in a Metglas strip to be 0.03% K-1. Using insights from theory, we then experimentally demonstrate a fivefold improvement to the TCF by using Terfenol in place of Metglas as the magnetostrictive sensor material. We further demonstrate an alternate temperature sensing technique that does not require measuring the resonance frequency, consequently reducing instrument complexity. This work provides a general framework to analyze magnetostrictive materials and the sensing scheme for near-field wireless thermometry.Powder bed additive manufacturing (AM) processes, including binder jetting (BJAM) and powder bed fusion (PBF), can manufacture complex three-dimensional components from a variety of materials. A fundamental understanding of the spreading of thin powder layers is essential to develop robust process parameters for powder bed AM and to assess the influence of powder feedstock characteristics on the subsequent process outcomes. Toward meeting these needs, this work presents the design, fabrication, and qualification of a testbed for modular, mechanized, multi-layer powder spreading. The testbed is designed to replicate the operating conditions of commercial AM equipment, yet features full control over motion parameters including the translation and rotation of a roller spreading tool and precision motion of a feed piston and the build platform. The powder spreading mechanism is interchangeable and therefore can be customized, including the capability for dispensing of fine, cohesive powders using a vibrating hopper. Validation of the resolution and accuracy of the machine and its subsystems, as well as the spreading of exemplary layers from a range of powder sizes typical of BJAM and PBF processes, are described. The precision engineered testbed can therefore enable the optimization of powder spreading parameters for AM and correlation to build process parameters in future work, as well as exploration of spreading of specialized powders for AM and other techniques.We have succeeded in operating a transition-edge sensor (TES) spectrometer and evaluating its performance at the SPring-8 synchrotron x-ray light source. The TES spectrometer consists of a 240 pixel National Institute of Standards and Technology (NIST) TES system, and 220 pixels are operated simultaneously with an energy resolution of 4 eV at 6 keV at a rate of ∼1 c/s pixel-1. The tolerance for high count rates is evaluated in terms of energy resolution and live time fraction, leading to an empirical compromise of ∼2 × 103 c/s (all pixels) with an energy resolution of 5 eV at 6 keV. By utilizing the TES's wideband spectroscopic capability, simultaneous multi-element analysis is demonstrated for a standard sample. We conducted x-ray absorption near-edge structure (XANES) analysis in fluorescence mode using the TES spectrometer. The excellent energy resolution of the TES enabled us to detect weak fluorescence lines from dilute samples and trace elements that have previously been difficult to resolve due to the nearly overlapping emission lines of other dominant elements. The neighboring lines of As Kα and Pb Lα2 of the standard sample were clearly resolved, and the XANES of Pb Lα2 was obtained. Moreover, the x-ray spectrum from the small amount of Fe in aerosols was distinguished from the spectrum of a blank target, which helps us to understand the targets and the environment. These results are the first important step for the application of high resolution TES-based spectroscopy at hard x-ray synchrotron facilities.Modern imaging techniques increasingly require signals to be collected from multiple viewpoints and spectral bands to realize multi-dimensional and multi-species detections. For this purpose, multiple cameras are commonly required. Each camera collects signals from one viewpoint or one spectral band, resulting in a considerable experimental cost. Based on frequency modulation, this work proposes an encoded-imaging technique that can record multangular and multispectral images in one acquisition. The signals recorded from different viewpoints and spectral bands are superimposed in the spatial domain, while being separate in the frequency domain. This allows us to extract individual images based on their respective frequency components. In this work, a proof-of-concept experiment was conducted. The high correlation coefficient between the superimposition of the extracted images and a normal superimposed image demonstrates the effectiveness of this technique. In addition, an improved mathematical formulation was proposed to describe the higher spatial-frequency components, which were considered merely to be residual lines in previous studies. The proposed encoded-imaging technique may have potential for multangular and multispectral imaging, which is especially useful for tomographic reconstructions.We present a laboratory electromagnet capable of generating magnetic fields up to ±0.48 T, specifically designed as a perpendicular flux source for thin film samples in an ambient environment. The magnet features a 250 mm diameter clear access bore above the sample plane, thus offering compatibility with a wide variety of experimental apparatus. Despite its generous size, the magnet thermally dissipates less than 1 kW at maximum field. A shaped ferromagnetic core is used to amplify and homogenize the field B, leading to an estimated uniformity of ±1.5 mT (≲0.3%) in B within a 28 mm2 zone at maximum field. The sample stage is thermally regulated and isolated from the magnet, enabling temperature control with ±5 mK precision even at elevated magnetic fields.

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