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optimal method for LtEc purification.Metabolomics involvement in the study of foods is steadily growing. Such a rise is a consequence of the increasing demand in the food sector to address challenges regarding the issues of food safety, quality, and authenticity in a more comprehensive way. Virgin olive oil (VOO) is a key product of the Mediterranean diet, with a globalized consumer interest as it may be associated with various nutritional and health benefits. Despite the strict legislation to protect this high added-value agricultural commodity and offer guarantees to consumers and honest producers, there are still analytical issues needing to be further addressed. Thus, this review aims to present the efforts made using targeted and untargeted metabolomics approaches, namely nuclear magnetic resonance (NMR) spectroscopy and mass spectrometry-based techniques (mainly LC/GC-MS) combined with multivariate statistical analysis. Case-studies focusing on geographical/varietal classification and detection of adulteration are discussed with regards to the identification of possible markers. The advantages and limitations of each of the aforementioned techniques applied to VOO analysis are also highlighted.Twenty Dorper × Katahdin male lambs (body weight = 33.9 ± 0.4 kg and age = 4.5 months) were individually housed for a 30-d feeding period to evaluate the effects of seasonal heat stress (winter [n = 10] vs. summer [n = 10]) on feedlot performance, carcass traits, wholesale cut yields and meat quality. Heat stress environmental conditions prevailed in summer and mostly thermoneutral in winter. Overall growth rate and feed efficiency, as well as empty body weight at slaughter, cold carcass weight, omental fat percentage, and loin yield were lower in summer than in winter. Kidney-pelvic-heart fat deposition and yields of hot carcass, neck and shoulder increased during summer. Postmortem aging of meat during 14 d exhibited higher lightness, redness, yellowness and toughness in summer. In conclusion, summer heat stress decreased growth and feed efficiency without affecting feed intake of hair male lambs. Additionally, heat stress improved carcass yield with no detrimental changes on meat quality.Waste sorting is essential to address the current predicament of waste management. Though it is important, insufficient attention has been paid to explore residents' waste sorting intention and behavior and understand its formation process. To narrow the research gap, this research built a theoretical research model by adding personal moral norms and waste sorting knowledge into the theory of planned behavior to explicate residents' waste sorting intention and behavior formation process. Meanwhile, given the discrepancy between waste sorting intention and actual behavior, this research also explored the effect of external conditions, such as incentive measures, on this discrepancy. Based on survey data from 397 Chinese residents, this research found that attitudes, subjective norms, perceived behavioral control, personal moral norms and waste sorting knowledge were directly and significantly related to residents' waste sorting intention. [https://www.selleckchem.com/products/TW-37.html TW-37] Waste sorting knowledge also had an indirect influence on residents' waste sorting intention through attitudes and perceived behavioral control. Additionally, this research corroborated the discrepancy between waste sorting intention and behavior, and suggested that the link between intention and behavior was contingent on incentive measures. Incentive measures strengthened the effect of intention on behavior. This research is useful for understanding residents' waste sorting intention and behavior and valuable for encouraging residents to sort waste in their daily lives.To recycle the sharply growing spent lithium-ion batteries and alleviate concerns over shortages of resources, particularly Li, is still an urgent issue. In this work, an organic acids based leaching approach at room temperature is proposed to recover Li and FePO4 from spent LiFePO4 cathode powder. The coexistent metal ions, Cu and Al, have also been investigated. Citrus fruit juices, rich in organic acids, such as citric acid and malic acid, have been used as leaching agents in this work. Among lemon, orange and apple, lemon juice shows the best leaching effect based on its suitable pH of the reaction system. Under the optimized conditions, the leaching rates of Li, Cu and Al can reach up to 94.83%, 96.92% and 47.24%, while Fe and P remain as low as 4.05% and 0.84%, respectively. Li2CO3 and FePO4 can be recovered from the leachate and the leaching residue, respectively. The recovered FePO4 was used to prepare new cathode material LiFePO4. The crystalline carbon, present in the spent LiFePO4 cathode scraps, has a significant effect on the electrochemical performances of the regenerated LiFePO4. The regenerated LiFePO4 cathode material delivered a comparable discharge capacity of 155.3 mAh g-1 at 0.1C and rate capacity to the fresh LiFePO4. For the cycling stability, it displays capacity retention of 98.30% over 100 cycles at 1 C with a fading rate of 0.017% per cycle. The proposed organic acids-based recycling strategy is much benign for recycling the spent LiFePO4 cathode materials.Mechanical biological treatment (MBT) approaches are being adopted to manage residual municipal waste (RMW) to promote the prevention or reduction of potential environmental impacts of landfilling. From this perspective, the present study aimed to increase the knowledge of the biological (anaerobic) stability of different MBT organic outputs and, conversely, initial methane generation from residual organic waste. Biochemical methane potential (BMP) tests, along with initial and final characterisations of substrates and digestates, were conducted on a mechanically separated organic fraction from RMW (ms-OFRMW); a first MBT organic output represented by a biostabilised organic fraction from RMW (bios-OFRMW); and a different MBT organic output represented by a biodried fine fraction from RMW (biod-FFRMW). The ms-OFRMW had a BMP of 445.6 Nml CH4 g VS-1, which was comparable or even higher than those from separately collected and source-sorted organic fractions. The fibre and liquor fractions of the digestate from ms-OFRMW with inoculum showed potential profiles of P-rich amendment and N-rich fluid phase, respectively, even satisfying environmental limits (with the exclusion only of Cu and Zn contents in fibre fraction that, however, remained within typical ranges for agricultural digestates).